HRID977891

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID19966045

未命名化合物

结构：CC(C)(C)c1ccc(CCC(CC2CCCCC2)O[Si](C)(C)C(C)(C)C)cc1N

HCID19966217

未命名化合物

PRODUCTS

生成物

结构：CC(C)(C)c1ccc(CCC(CC2CCCCC2)O[Si](C)(C)C(C)(C)C)cc1NC(=O)CC1(c2ccccc2)CCCC1

HCID19966114

未命名化合物

PROCEDURE

实验过程

Following a procedure similar to that described in Example 21, but using 2-(1-phenylcyclopentyl)acetic acid [prepared as described in Preparation 21] and 2-t-butyl-5-[4-cyclohexyl-3-(t-butyldimethylsilyloxy)butyl]aniline [prepared by a procedure similar to that described in Preparation 11(i)] as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained as a foam-like material.

WORKUP

后处理

customprepared by a procedure similar to

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-51c15e470b5349ea82df656f51c82323
来源数据集: uspto-grants-1997_03
DOI: 10.6084/m9.figshare.5104873.v1
专利: US05614550
来源说明: uspto-grants-1997_03

反应 SMILES

[C:1]1([C:7]2([CH2:12][C:13]([OH:15])=O)[CH2:11][CH2:10][CH2:9][CH2:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:16]([C:20]1[CH:26]=[CH:25][C:24]([CH2:27][CH2:28][CH:29]([O:37][Si:38]([C:41]([CH3:44])([CH3:43])[CH3:42])([CH3:40])[CH3:39])[CH2:30][CH:31]2[CH2:36][CH2:35][CH2:34][CH2:33][CH2:32]2)=[CH:23][C:21]=1[NH2:22])([CH3:19])([CH3:18])[CH3:17]>>[C:16]([C:20]1[CH:26]=[CH:25][C:24]([CH2:27][CH2:28][CH:29]([O:37][Si:38]([C:41]([CH3:44])([CH3:43])[CH3:42])([CH3:40])[CH3:39])[CH2:30][CH:31]2[CH2:32][CH2:33][CH2:34][CH2:35][CH2:36]2)=[CH:23][C:21]=1[NH:22][C:13](=[O:15])[CH2:12][C:7]1([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[CH2:8][CH2:9][CH2:10][CH2:11]1)([CH3:19])([CH3:17])[CH3:18]