HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(1-Phenylcyclopentyl)acetic acid → N-{2-t-Butyl-5-[4-cyclohexyl-3-(t-butyldimethylsilyloxy)butyl]phenyl}-2-(1-phenylcyclopentyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(1-Phenylcyclopentyl)acetic acid | HCID 19966045 | — |
| Reactant | 2-t-Butyl-5-[4-cyclohexyl-3-(t-butyldimethylsilyloxy)butyl]aniline | HCID 19966217 | — |
| Product | N-{2-t-Butyl-5-[4-cyclohexyl-3-(t-butyldimethylsilyloxy)butyl]phenyl}-2-(1-phenylcyclopentyl)acetamide | HCID 19966114 | — |
Reaction Steps
Following a procedure similar to that described in Example 21, but using 2-(1-phenylcyclopentyl)acetic acid [prepared as described in Preparation 21] and 2-t-butyl-5-[4-cyclohexyl-3-(t-butyldimethylsilyloxy)butyl]aniline [prepared by a procedure similar to that described in Preparation 11(i)] as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained as a foam-like material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05614550 |
| Source dataset | uspto-grants-1997_03 |
| ORD ID | ord-51c15e470b5349ea82df656f51c82323 |
| Source note | uspto-grants-1997_03 |