HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → HCID 9794284, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 9794284 | HCID 9794284 | 76.2% |
Reaction Steps
Phenethylamine (121 g) is dissolved in methanol (500 ml) and thereto is added dropwise methyl acrylate (86 g) at room temperature. The mixture is stirred for 4 hours and then distilled to remove the solvent to give N-phenethyl-β-alanine methyl ester (157.8 g, 76%), b.p. 124°-127° C. (1.2 mmHg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04663319 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-f0ba5c3e23e14822b993c43074aa7818 |
| Source note | uspto-grants-1987_05 |