HRID977958

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6340

Ethane, iodo-

C2H5I

结构：CCOC(=O)C1CN(Cc2ccccc2)C(=O)C(=C2SC=CS2)C1=O

HCID13934862

未命名化合物

PRODUCTS

生成物

结构：CCOC(=O)C1(CC)CN(Cc2ccccc2)C(=O)C(=C2SC=CS2)C1=O

HCID20204024

未命名化合物

收率 79.3%

PROCEDURE

实验过程

Ethyl 1-benzyl-5-(1,3-dithiol-2-ylidene)-4.6-dioxopiperidine-3-carboxylate (2.70 g) and ethyl iodide (0.71 ml) are treated in the same manner as described in Example 25-(1), whereby ethyl 1-benzyl-5-(1,3-dithiol-2-ylidene)-3-ethyl-4,6-dioxopiperidine-3-carboxylate (2.30 g, 79.3%) is obtained as pale yellow oil.