HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 7-(Dimethylamino)hept-5-ynylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | N-(5-Hexynyl)phthalimide | HCID 3346053 | — |
| Product | 7-(Dimethylamino)hept-5-ynylamine | HCID 20147646 | — |
Reaction Steps
In a manner similar to Description 1 (iii) and (iv) reaction of N-5-hexynylphthalimide, paraformaldehyde and dimethylamine, followed by treatment with hydrazine hydrate gave the title compound b.p. 110°-20° C. (0.3 mm Hg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04663331 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-508f477bc9734dd6883f26d90d9dfd96 |
| Source note | uspto-grants-1987_05 |