HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Di-tert-butyl-4-mercaptophenol → 3-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]thio]-N-ethyl-N-(4-pyridinylmethyl)propanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Reactant | HCID 19826117 | HCID 19826117 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 3-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]thio]-N-ethyl-N-(4-pyridinylmethyl)propanamide | HCID 13822940 | — |
Reaction Steps
The title compound was prepared according to the method of Example 4 from N-ethyl-N-(4-pyridinylmethyl)-2-propenamide (1.5 g, 0.00788 mole,), 2,6-bis(1,1-dimethyl-ethyl)-4-mercaptophenol (2.06 g, 0.00867 mole,) and triethylamine (1 ml) to provide 3.0 g of product, m.p. ca. 121°-123° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04663333 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-19080efa9db246d594b87d4ee6166208 |
| Source note | uspto-grants-1987_05 |