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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 978001Generated: October 30, 2026

2,6-Di-tert-butyl-4-mercaptophenol → 3-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]thio]-N-ethyl-N-(4-pyridinylmethyl)propanamide

https://huagongshe.com/reaction/978001

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,6-Di-tert-butyl-4-mercaptophenolHCID 70370—
ReactantHCID 19826117HCID 19826117—
SolventTriethylamineHCID 8471—
Product3-[[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]thio]-N-ethyl-N-(4-pyridinylmethyl)propanamideHCID 13822940—

Reaction Steps

The title compound was prepared according to the method of Example 4 from N-ethyl-N-(4-pyridinylmethyl)-2-propenamide (1.5 g, 0.00788 mole,), 2,6-bis(1,1-dimethyl-ethyl)-4-mercaptophenol (2.06 g, 0.00867 mole,) and triethylamine (1 ml) to provide 3.0 g of product, m.p. ca. 121°-123° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04663333
Source datasetuspto-grants-1987_05
ORD IDord-19080efa9db246d594b87d4ee6166208
Source noteuspto-grants-1987_05