HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazoic acid → HCID 178427292, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazoic acid | HCID 24530 | — |
| Reactant | p-Toluenesulphonyl cyanide | HCID 87946 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 178427292 | HCID 178427292 | — |
Reaction Steps
A mixture of p-toluenesulfonyl cyanide (0.0 g.) and excess hydrazoic acid in 50 ml. of benzene is stirred at room temperature for 20 hours. The product is filtered off, dissolved in ether, filtered through celite and evaporated to a solid which on trituration with benzene has a melting point, 133°-135° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04663461 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-af4679b8e3c64a1a8be2e3fe735041f1 |
| Source note | uspto-grants-1987_05 |