HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Dimethylamino)Benzaldehyde → HCID 86741481, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Dimethylamino)Benzaldehyde | HCID 7479 | — |
| Reactant | Bisulfite | HCID 104748 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86741481 | HCID 86741481 | — |
Reaction Steps
10 g. (0.067 mole) 4-Dimethylaminobenzaldehyde are dissolved in 50 ml. toluene and vigorously stirred for six hours with 100 ml. saturated bisulphite solution. The resulting crystalline material is filtered off with suction and washed with 50 ml. toluene. Yield: 12.8 g. (75% of theory).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04665023 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-b2aae14a8eff4ca4b5913b250ecac645 |
| Source note | uspto-grants-1987_05 |