HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → 1H-Imidazole, 1-(1-oxohexyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | Hexanoyl chloride | HCID 67340 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 1H-Imidazole, 1-(1-oxohexyl)- | HCID 10920880 | — |
Reaction Steps
The method of Pfander and Laederach [H. Pfander and M. Laederach, Carbohyd. Res. 99(2), 175-79 (1982)] was used. 1-Hexanoylimidazole was prepared by stirring 2 equivalents of imidazole with 1 equivalent hexanoyl chloride in toluene solution. The mixture was filtered and concentrated to a low-melting solid. This product, 1-hexanoylimidazole, was further purified by distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04665057 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-a52b058a9a9f42f8b49af0aa6486c189 |
| Source note | uspto-grants-1987_05 |