HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → (1-Methyl-1-ethylpropylamino)ethoxyethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 3-Methylpentan-3-amine | HCID 4339626 | — |
| Reactant | 2-Chloroethoxyethanol | HCID 22145445 | — |
| Solvent | 2-Methoxyethanol | HCID 8019 | — |
| Product | (1-Methyl-1-ethylpropylamino)ethoxyethanol | HCID 86739621 | — |
Reaction Steps
A solution of 124.7 g of 1-methyl-1-ethylpropylamine and 76.9 g of 2-chloroethoxyethanol in 300 ml of ethylene glycol monomethylether was refluxed overnight. The reaction mixture was treated with a stoichiometric excess of KOH and refluxed for one hour, filtered, and distilled. The product had a b.p. of 153° C. (2 mm). Analysis calculated for C10H23NO2 :% N, 7.4, found %N, 7.15.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04665234 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-e8016256d9004eda802daf757106c1d7 |
| Source note | uspto-grants-1987_05 |