HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20201103, compound → 4-Methyl-2-(methylsulfanyl)thiophen-3-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20201103 | HCID 20201103 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 4-Methyl-2-(methylsulfanyl)thiophen-3-amine | HCID 20201109 | — |
Reaction Steps
6 g (0.22 gram atoms) freshly prepared aluminium amalgam are added over a period of about two minutes to 18.9 g (0.1 mol) of 2-methylthio-4-methyl-3-nitrothiophene dissolved in 200 ml of moist diethylether. The vigorous reaction which sets in after 5-10 minutes is kept under control by cooling the flask in ice.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04666502 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-dfa6b5a73c394992a319395e4b4c1656 |
| Source note | uspto-grants-1987_05 |