HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20201113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 20201086 | HCID 20201086 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20201113 | HCID 20201113 | — |
Reaction Steps
To 12.25 g (0.066 mol) of methyl 3,5-dimethyl-4-aminothiophene-2-carboxylate, 9.1 g (0.066 mol) of K2CO3, 25 ml of water and 150 ml of methylene chloride are added without cooling 7.5 g (0.066 mol) of chloroacetyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04666502 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-c555b0af5c9e462a925970d878737fde |
| Source note | uspto-grants-1987_05 |