HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → 2-Chloro-N-(5-chloro-2,4-dimethylthiophen-3-yl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | N-(2,4-Dimethylthien-3-yl)-chloroacetamide | HCID 20201107 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Chloro-N-(5-chloro-2,4-dimethylthiophen-3-yl)acetamide | HCID 20201095 | — |
Reaction Steps
To the stirred solution of 5.0 g (0.0245 mol) of N-(2,4-dimethylthien-3-yl)-chloroacetamide in 50 ml of dry CH2Cl2 are added dropwise at 0° 3.3 g (0.0245 mol) of sulfuryl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04666502 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-32dca15284224d2a95fe9600b582abdb |
| Source note | uspto-grants-1987_05 |