HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Pyrazole-4-carboxylic acid, 5-(aminocarbonyl)-1-(3-chlorophenyl)- → HCID 178449045, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Pyrazole-4-carboxylic acid, 5-(aminocarbonyl)-1-(3-chlorophenyl)- | HCID 163715 | — |
| Reactant | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178449045 | HCID 178449045 | — |
Reaction Steps
A 3.26 g. portion of 4-carboxy-1-(3-chlorophenyl)-5-pyrazolecarboxamide was slurried in 50 ml. of methanol and 12 ml. of 1M tetrabutyl ammonium hydroxide solution was added. The mixture was stirred for 30 minutes, and evaporated to dryness under vacuum to obtain 5.2 g. of product, m.p. 120°-121°. The product was identified by elemental analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04666504 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-ed5095fedc5b46a4890db1f85ce5e7d9 |
| Source note | uspto-grants-1987_05 |