Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 86741509 | HCID 86741509 | — |
| Product | HCID 13576359 | HCID 13576359 | — |
Reaction Steps
4.7 g (0.026 mol) of 4-(2-furyl)-carbonyl-γ-butyrolactone and 1.5 ml (0.03 mol) of hydrazine hydrate are dissolved in 40 ml of ethanol at room temperature and stirred at 50° C. for 1 hour. After the mixture has been concentrated, the reaction product is subjected to fractionation by chromatography over a silica gel column using methylene chloride/methanol=9:1 as the mobile phase.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04666902 |
|---|
| Source dataset | uspto-grants-1987_05 |
|---|
| ORD ID | ord-57fa37f41e6d4fa0a18ba98839dafcae |
|---|
| Source note | uspto-grants-1987_05 |
|---|
