Diethyl Ether → HCID 13576363, compound

Participants

Reaction Steps

5.2 g (0.017 mol) of 4-(4-(2-(1-imidazolyl)-ethoxy)phenyl)-carbonyl-γ-butyrolactone and 1 ml (0.02 mol) of hydrazine hydrate are stirred in 30 ml of ethanol at room temperature for 1 hour and then at 60° C. for 16 hours. After the mixture has been cooled, 15 ml of ether are added and the precipitated product is filtered off with suction, washed with either and dried.

Provenance & Evidence