Ethanol → HCID 13576366, compound

HRID 979037Notes

Reaction equation

HRID 979037 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][O:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]([CH:14]2OC(=O)[CH2:16][CH2:15]2)=O)=[CH:8][CH:7]=1.[OH2:20].[NH2:21][NH2:22].[CH2:23]([OH:25])C>>[CH3:1][O:2][CH2:3][CH2:4][O:5][C:6]1[CH:7]=[CH:8][C:9]([C:12]2[CH:14]([CH2:23][OH:25])[CH2:15][C:16](=[O:20])[NH:21][N:22]=2)=[CH:10][CH:11]=1

Participants

4

Reactant 3

HCID 702EthanolHCID 24654Hydrazine hydrate (1:1)HCID 20201504HCID 20201504, compound

Product 1

HCID 13576366HCID 13576366, compound

Procedure

13.7 g (0.052 mol) of 4-(4-(2-methoxyethoxy)-phenyl-carbonyl)-γ-butyrolactone are reacted with 2.8 g (0.056 mol) of hydrazine hydrate in 80 ml of ethanol as described above.

Sources & evidence

ORD record
ord-6a4cd7c44a1641748238752887da4e2c
Source dataset
uspto-grants-1987_05
Patent number
US04666902

Reaction notes

Loading…