HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 13576369, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 86741516 | HCID 86741516 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13576369 | HCID 13576369 | — |
Reaction Steps
10.6 g (0.045 mol) of 4-(4-methylmercaptophenyl)-carbonyl-γ-butyrolactone are stirred in 70 ml of ethanol with 2.5 g (0.05 mol) of hydrazine hydrate at room temperature for 90 minutes. After addition of 8 ml of acetic acid, the mixture is heated under reflux for 1 hour and cooled and the precipitate is filtered off with suction and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04666902 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-0731e8e6ecad40ad99af0a23006cf2f6 |
| Source note | uspto-grants-1987_05 |