Ethanol → HCID 13576371, compound

HRID 979039Notes

Reaction equation

HRID 979039 reaction equation
[NH2:1][C:2]([CH2:4][O:5][C:6]1[CH:11]=[CH:10][C:9]([CH:12]2OC(=O)[C:14](=[C:18]=[O:19])[CH2:13]2)=[CH:8][CH:7]=1)=[O:3].O.[NH2:21][NH2:22].[CH2:23]([OH:25])C>>[NH2:1][C:2]([CH2:4][O:5][C:6]1[CH:7]=[CH:8][C:9]([C:12]2[CH:13]([CH2:23][OH:25])[CH2:14][C:18](=[O:19])[NH:21][N:22]=2)=[CH:10][CH:11]=1)=[O:3]

Participants

4

Reactant 3

HCID 702EthanolHCID 24654Hydrazine hydrate (1:1)HCID 86741517HCID 86741517, compound

Product 1

HCID 13576371HCID 13576371, compound

Procedure

11.3 g (0.043 mol) of 4-(4-(aminocarbonylmethoxy)-phenyl)-carbonyl-γ-butyrolactone and 2.4 g (0.048 mol) of hydrazine hydrate are reacted in 70 ml of ethanol, as described above.

Sources & evidence

ORD record
ord-92dd6cd774ea42af895d95cf942ed465
Source dataset
uspto-grants-1987_05
Patent number
US04666902

Reaction notes

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