Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 131715139 | HCID 131715139 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13576373 | HCID 13576373 | — |
Reaction Steps
3.0 g (0.014 mol) of 4-(4-cyanophenyl)-carbonyl-γ-butyrolactone and 1 ml (0.021 mol) of hydrazine hydrate are stirred in 50 ml of ethanol and 50 ml of dimethylformamide at room temperature for 10 hours. After addition of 1 ml of acetic acid, the mixture is stirred at 80° C. for 18 hours and worked up as above.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04666902 |
|---|
| Source dataset | uspto-grants-1987_05 |
|---|
| ORD ID | ord-7bc602a621804732a5beb7d125085104 |
|---|
| Source note | uspto-grants-1987_05 |
|---|
