HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 979084Generated: October 31, 2026
Hydrogen Peroxide → 4-chloro-3-methoxy-10-methyl-5-oxo-10H-phenothiazine
https://huagongshe.com/reaction/979084
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | 4-chloro-3-methoxy-10-methyl-10H-phenothiazine | HCID 13882027 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 4-chloro-3-methoxy-10-methyl-5-oxo-10H-phenothiazine | HCID 13882072 | — |
Reaction Steps
To 4-chloro-3-methoxy-10-methyl-10H-phenothiazine (0.5 g) (see Example 5) was added acetic acid (12 ml) and hydrogen peroxide (2 ml). The reaction mixture was heated at 50° C. for 15 minutes and then, evaporated to dryness. The corresponding sulfoxide (0.5 g) (4-chloro-3-methoxy-10-methyl-5-oxo-10H-phenothiazine) was obtained by crystallization (m.p. decomposed at 141° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04666907 |
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| Source dataset | uspto-grants-1987_05 |
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| ORD ID | ord-f54d01d90ec04bcfa984328e5404f99b |
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| Source note | uspto-grants-1987_05 |
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