HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 178422930, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 178422932 | HCID 178422932 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178422930 | HCID 178422930 | 100.7% |
Reaction Steps
4-(3-Methyl-4-nitrophenyl)-1-H-imidazole (9.2 g) was allowed to react with 85% hydrazine hydrate in methanol to give 7.9 g of 4-(3-methyl-4-aminophenyl)-1-H-imidazole, M.p. 195°-197° C. 4-(3-Methoxy-4-aminophenyl)-1-H-imidazole, M.p. 145° C. (dec.), was prepared analogously.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04666932 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-91fe6d01ed704010af0a529ea394a7ce |
| Source note | uspto-grants-1987_05 |