2-Methoxyethylamine → HCID 178495956, compound

HRID 979195Notes

Reaction equation

HRID 979195 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][NH2:5].C(N[CH:9]=[N:10][C:11]1[CH:16]=[CH:15][C:14]([C:17]2[N:18]=[CH:19][NH:20][CH:21]=2)=[CH:13][CH:12]=1)#N>O>[CH3:1][O:2][CH2:3][CH2:4][NH:5][CH:9]=[N:10][C:11]1[CH:16]=[CH:15][C:14]([C:17]2[N:18]=[CH:19][NH:20][CH:21]=2)=[CH:13][CH:12]=1

Participants

4

Reactant 2

HCID 80182-MethoxyethylamineHCID 178512241HCID 178512241, compound

Product 1

HCID 178495956HCID 178495956, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

5 ml of 2-methoxy-ethylamine were added all at once to a suspension of N-cyano-N'-[4-(imidazol-4-yl)-phenyl]-formamidine (1.8 g) in water (2 ml). When the exothermic reaction subsided, a solution was obtained from which the title compound quickly crystallized out. The product was filtered off and purified via its maleate in acetone.

Workup

  1. customWhen the exothermic reaction

Sources & evidence

ORD record
ord-694a6a6d837d489abe5fab3870b41edf
Source dataset
uspto-grants-1987_05
Patent number
US04666932

Reaction notes

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