HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2,2-Trichloroethyl hydrazinecarboxylate → HCID 131715142, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2,2-Trichloroethyl hydrazinecarboxylate | HCID 13688509 | — |
| Reactant | HCID 87750519 | HCID 87750519 | — |
| Product | HCID 131715142 | HCID 131715142 | 46.4% |
Reaction Steps
According to the process of H. Watanabe et al, Chemical Pharmaceutical Bulletin, vol. 22, p. 1889 (1974), 4 g of Gln(OMe) is reacted with 4 g of β,β,β-trichloroethyloxycarbonylhydrazine (hereinafter referred to as "TrocNHNH2 ") to obtain 3 g of GlnNHNH-Troc.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04667017 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-593b03db55ac414281a9068fb47add93 |
| Source note | uspto-grants-1987_05 |