Hydrazine hydrate (1:1) → HCID 13370245, compound

HRID 979282Notes

Reaction equation

HRID 979282 reaction equation
[N:1]1([CH2:6][C:7]2[S:11][C:10]([C:12](=O)[CH2:13][CH2:14][C:15]([OH:17])=O)=[CH:9][CH:8]=2)[CH:5]=[CH:4][CH:3]=[N:2]1.O.[NH2:20][NH2:21]>O>[N:1]1([CH2:6][C:7]2[S:11][C:10]([C:12]3[CH2:13][CH2:14][C:15](=[O:17])[NH:20][N:21]=3)=[CH:9][CH:8]=2)[CH:5]=[CH:4][CH:3]=[N:2]1

Participants

4

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 13370248HCID 13370248, compound

Product 1

HCID 13370245HCID 13370245, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Analoguous to Example 2(b), the reaction is carried out with 29 g of 4-[5-(pyrazol-1-yl-methyl)-thien-2-yl]-4-oxo-butyric acid and 6.6 g of hydrazin hydrate in 100 ml water.

Sources & evidence

ORD record
ord-cbe2722bfeda4cd699c53ad446e38e99
Source dataset
uspto-grants-1987_05
Patent number
US04667033

Reaction notes

Loading…