HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 13853731, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 12199928 | HCID 12199928 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 13853731 | HCID 13853731 | — |
Reaction Steps
To a suspension of 1,7-dimethoxy-3H-phenothiazin-3-one (300 mg) in acetic acid (9 ml) was added a 0.63M solution of Br2 in acetic acid (1.92 ml). After 15 minutes, methanol was added and the solid filtered, washed with ether and air dried to afford the title compound (353 mg), m.p. 267°-270° C. (dec).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04667032 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-933d288bd42b4593a7a4458eb5a2bf74 |
| Source note | uspto-grants-1987_05 |