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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 979341Generated: October 30, 2026

Potassium Carbonate → HCID 13689403, compound

https://huagongshe.com/reaction/979341

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant11-(piperdin-4-yl)-5H,11H-pyrrolo[2,1-c][1,4]benzoxazepineHCID 13689358—
ReactantHCID 54410630HCID 54410630—
SolventDimethylformamideHCID 6228—
ProductHCID 13689403HCID 13689403—

Reaction Conditions

Temperature65 °C

Reaction Steps

A mixture of 11-(piperidin-4-yl)-5H,11H-pyrrolo[2,1-c][1,4]benzoxazepine (6.15 g, 0.023 mole), 2-(3-trifluoromethylphenyl)ethyl menthanesulfonate (7.27 g, 0.027 mole) and K2CO3 (10.6 g) in 125 ml dimethylformamide was heated at 65° C. for 5 hours.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04667039
Source datasetuspto-grants-1987_05
ORD IDord-43c97d6636ac4101acc5cc375cdf2f73
Source noteuspto-grants-1987_05