HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 129140, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 86741541 | HCID 86741541 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 129140 | HCID 129140 | 108.1% |
Reaction Steps
5 g of (+)-6-Chloro-5,10-dihydro-5-[(1-methyl-4-piperidinyl)-acetyl] -11H-dibenzo[b,e][1,4]diazepin-11-one-L-(+)-tart rate were dissolved in water, mixed with potash and extracted with methylene chloride. The extracts were combined and evaporated off several times with ethanol. 3.9 g (95% of theory) of (+)-6-chloro-5,10-dihydro-5-[(1-methyl-4-piperidinyl)-acetyl]-11H-dibenzo[b,e][1,4]diazepin-11-one were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04668674 |
| Source dataset | uspto-grants-1987_05 |
| ORD ID | ord-5ef814044a9e4b73b02d6fbdad4ca47c |
| Source note | uspto-grants-1987_05 |