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HRID979694

反应详情

EQUATION

反应方程式

HRID 979694 的结构方程式

REACTANTS

反应物

2
结构：C=C[Si](OC(C)C)(OC(C)C)OC(C)C
HCID87409

Silane, ethenyltris(1-methylethoxy)-

C11H24O3Si

结构：CC(C)(C)O[SiH](OC(C)(C)C)OC(C)(C)C
HCID101075511

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)O[Si](C=C[Si](OC(C)(C)C)(OC(C)(C)C)OC(C)(C)C)(OC(C)C)OC(C)C
HCID54208286

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1C
溶剂HCID7237

o-Xylene

C8H10

CONDITIONS

反应条件

温度
225 °C

PROCEDURE

实验过程

Into a 45 cc Parr bomb was added 2.5 g (0.010 mol) tritertbutoxysilane, 4.7 g (0.020 mol) vinyltriisopropoxysilane, 1.0 g xylene and 2000 ppm Ru3CO12 (29 mg) as a catalyst. The reaction was heated to 225° C. for 3 hours in a fluidized sand bath. A single product, 1-tritertbutoxysilyl-2-triisopropoxysilylethylene was formed.