HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 979694Generated: October 25, 2026
Silane, ethenyltris(1-methylethoxy)- → 1-Tritertbutoxysilyl-2-triisopropoxysilylethylene
https://huagongshe.com/reaction/979694
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Silane, ethenyltris(1-methylethoxy)- | HCID 87409 | — |
| Reactant | Tris(tert-butoxy)silane | HCID 101075511 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | 1-Tritertbutoxysilyl-2-triisopropoxysilylethylene | HCID 54208286 | — |
Reaction Steps
Into a 45 cc Parr bomb was added 2.5 g (0.010 mol) tritertbutoxysilane, 4.7 g (0.020 mol) vinyltriisopropoxysilane, 1.0 g xylene and 2000 ppm Ru3CO12 (29 mg) as a catalyst. The reaction was heated to 225° C. for 3 hours in a fluidized sand bath. A single product, 1-tritertbutoxysilyl-2-triisopropoxysilylethylene was formed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04668812 |
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| Source dataset | uspto-grants-1987_05 |
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| ORD ID | ord-ce0c828dc6334923bb02036296c792c4 |
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| Source note | uspto-grants-1987_05 |
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