HRID979704
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
A mixture of 17g (0.15 mole) allyl diethyl amine and 30.7g (0.165 mole, 10% excess) of diphenyl phosphine is reacted in the usual manner with u.v. irradiation for hours. A subsequent analysis of the reaction mixture indicated that about one third of the reactants was converted. The only product formed was the desired adduct, 2-diethylaminopropyl diphenylphosphine. It was isolated as a clear colorless liquid (Table 3).
WORKUP
后处理
- customis reacted in the usual manner with u.v
- customirradiation for hours
- customThe only product formed
- customIt was isolated as a clear colorless liquid (Table 3)