HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → Hydrogen Peroxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Hexanoic acid, 6-[(1-oxononyl)amino]- | HCID 11022006 | — |
| Solvent | Methanesulfonic Acid | HCID 6395 | — |
| Product | Hydrogen Peroxide | HCID 784 | — |
| Product | Hexanoic acid, 6-[(1-oxononyl)amino]- | HCID 11022006 | — |
| Product | HCID 17979835 | HCID 17979835 | — |
Reaction Steps
N-nonanoyl-6-aminoperoxycaproic acid was prepared by reaction of N-nonanoyl-6-aminocaproic acid with hydrogen peroxide in 98% methanesulfonic acid according to the procedure described in Example II. From 103 g (0.381 mol) of N-nonanoyl-6-aminocaproic acid, 44 g (1.29 mol) of hydrogen peroxide, and 170 mL of methanesulfonic acid was obtained 74.2 g of N-nonanoyl-6-aminoperoxycaproic acid having a peroxyacid AvO of 5.31% and a mp of 60° C. (theoretical yield=109.5 g of 5.57% AvO).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04634551 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-5ddda3fa1c4b492094fe74216d8f180f |
| Source note | uspto-grants-1987_01 |