Benzyl Alcohol → Benzyl 2-mercaptopropanoate

HRID 979763Notes

Reaction equation

HRID 979763 reaction equation
[CH2:1]([OH:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[SH:9][CH:10]([CH3:14])[C:11](O)=[O:12].C1(C)C=CC(S(O)(=O)=O)=CC=1>>[CH2:1]([O:8][C:11](=[O:12])[CH:10]([SH:9])[CH3:14])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 3

HCID 244Benzyl AlcoholHCID 6101p-Toluenesulfonic acidHCID 62326(+-)-2-Mercaptopropionic acid

Product 1

HCID 10442670Benzyl 2-mercaptopropanoate

Procedure

Into a 100 ml reaction flask equipped with thermometer, reflux condenser, hot plate (equipped with magnetic stirring apparatus) and spin bar are placed 21.6 grams benzyl alcohol; 29.6 grams of 2-mercaptopropionic acid; and 0.5 grams of para-toluene sulphonic acid.

Workup

  1. customInto a 100 ml reaction flask
  2. customequipped with thermometer
  3. temperaturereflux condenser
  4. customhot plate (equipped with magnetic stirring apparatus)

Sources & evidence

ORD record
ord-ac0f45cdaa544d538806cccefe995c8a
Source dataset
uspto-grants-1987_01
Patent number
US04634595

Reaction notes

Loading…