HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 70434270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 20222960 | HCID 20222960 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 70434270 | HCID 70434270 | 80% |
Reaction Steps
A solution of the product from Example 77 (2.5 g) in pyridine (10 ml) was treated with methanesulfonyl chloride (2 ml). After 4 hours stirring at room temperature the reaction was diluted with water and the mixture was filtered and dried affording 2.76 of product (80% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04634705 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-1aa087899d6c49db8dbfa649a279af1a |
| Source note | uspto-grants-1987_01 |