HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → 6-Amino-5-nitro-1-tetralone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 6-Acetamido-5-nitro-1-tetralone | HCID 14005224 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | 6-Amino-5-nitro-1-tetralone | HCID 14005226 | — |
Reaction Steps
The product from Example 81 (1 g) was treated with 6N hydrochloric acid (30 ml) at reflux for 2 hours and the reaction cooled then basified with ammonium hydroxide. The desired product was filtered, washed and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04634705 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-6c32b94f6dd94432b0b222811c94b446 |
| Source note | uspto-grants-1987_01 |