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HRID979812

反应详情

EQUATION

反应方程式

HRID 979812 的结构方程式

REACTANTS

反应物

2
结构：[NH4+].[OH-]
HCID14923

Ammonium hydroxide

H5NO

结构：CC(=O)Nc1ccc2c(c1[N+](=O)[O-])CCCC2=O
HCID14005224

未命名化合物

PRODUCTS

生成物

1
结构：Nc1ccc2c(c1[N+](=O)[O-])CCCC2=O
HCID14005226

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cl
溶剂HCID313

Hydrochloric Acid

ClH

PROCEDURE

实验过程

The product from Example 81 (1 g) was treated with 6N hydrochloric acid (30 ml) at reflux for 2 hours and the reaction cooled then basified with ammonium hydroxide. The desired product was filtered, washed and dried.

WORKUP

后处理

  1. temperatureat reflux for 2 hours
  2. temperaturethe reaction cooled
  3. filtrationThe desired product was filtered
  4. washwashed
  5. customdried