Tert-Butyl hypochlorite → HCID 20222972, compound

HRID 979816Notes

Reaction equation

HRID 979816 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][C:11]=1[CH3:12])[C:8](=[O:13])[CH2:7][CH2:6][CH2:5]2.[Cl:14]OC(C)(C)C>O1CCCC1>[NH2:1][C:2]1[C:3]([Cl:14])=[C:4]2[C:9](=[CH:10][C:11]=1[CH3:12])[C:8](=[O:13])[CH2:7][CH2:6][CH2:5]2

Participants

4

Reactant 2

HCID 521297Tert-Butyl hypochloriteHCID 20223006HCID 20223006, compound

Product 1

HCID 20222972HCID 20222972, compoundYield 90%

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

The product from Example 105 (0.175 g) was dissolved in tetrahydrofuran (5 ml) and was treated with t-butyl hypochlorite (0.12 ml). Following the procedure of Example 95 the desired product was obtained in 90% yield.

Sources & evidence

ORD record
ord-810634ec6dfa472abb3a38492e38a468
Source dataset
uspto-grants-1987_01
Patent number
US04634705

Reaction notes

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