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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 979820Generated: October 30, 2026

HCID 86741188, compound → HCID 20223040, compound

https://huagongshe.com/reaction/979820

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86741188HCID 86741188—
SolventHydrochloric AcidHCID 313—
ProductHCID 20223040HCID 20223040—

Reaction Conditions

Temperature0 °C

Reaction Steps

A solution of the product from Example 119 (0.38 g) in 6N hydrochloric acid (40 ml) was refluxed for 14 hours. The reaction mixture was cooled to 0° C., basified to pH 11 and extracted with methylene chloride. The organic layer was separated, dried and evaporated to afford the desired compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04634705
Source datasetuspto-grants-1987_01
ORD IDord-a4b88f7d27eb410f959ab6277836bc83
Source noteuspto-grants-1987_01