HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → N-(4-Aminocyclohexyl)-N'-ethylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | N-(4-Aminocyclohexyl)-N'-ethylurea--hydrogen chloride (1/1) | HCID 13755493 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N-(4-Aminocyclohexyl)-N'-ethylurea | HCID 13755492 | — |
Reaction Steps
A solution of 1.5 g of 1-(4-aminocyclohexyl)-3-ethylurea hydrochloride in 20 ml of methyl alcohol is treated with 0.36 g of sodium methoxide, to yield after usual workup 1-(4-aminocyclohexyl)-3-ethylurea as an oil which is used directly in the above condensation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04634713 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-7d56d3b0490c46be9553e42cbfec1836 |
| Source note | uspto-grants-1987_01 |