HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzylamine → HCID 20222900, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzylamine | HCID 67326 | — |
| Reactant | Isothiocyanatoacetaldehyde dimethyl acetal | HCID 144710 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20222900 | HCID 20222900 | 99% |
Reaction Steps
A mixture of 4.8 parts of 1-isothiocyanato-2,2-dimethoxyethane, 4.2 parts of 4-fluorobenzenemethanamine and 90 parts of tetrahydrofuran was stirred overnight. The reaction mixture was evaporated, yielding 8.9 parts (99%) of N-(2,2-dimethoxyethyl)-N'-[(4-fluorophenyl)methyl]thiourea (188).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04634704 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-9bd70976f211457cba8a73591c25974b |
| Source note | uspto-grants-1987_01 |