HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 86741194, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | 2-Methyl-1-pentanol | HCID 7745 | — |
| Reactant | Triisobutylaluminum | HCID 16682931 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | HCID 86741194 | HCID 86741194 | — |
Reaction Steps
To 10 ml of 1.085M DBM in heptane containing 0.33 ml of 0.92M TIBAL is added slowly a mixture of 2-methyl-1-pentanol (1.80 ml, 14.45 mmoles) and isopropanol (0.55 ml, 7.25 mmoles) diluted to 5 ml with cyclohexane. The solution remains clear throughout the addition (no precipitate formation) and is crystal-clear and somewhat viscous at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04634786 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-3e37218478134bd58e3d0133c36045c2 |
| Source note | uspto-grants-1987_01 |