HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 20222095, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Dazoxiben | HCID 53001 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 20222095 | HCID 20222095 | — |
Reaction Steps
Successive treatment of 1-[2-(4-carboxyphenoxy)ethyl]imidazole (1.4 g) with thionyl chloride (1.4 g) and morpholine (10 ml) as described in Example 25 gave N-[4-(2-imidazol-1-yl)ethoxybenzoyl]morpholine, m.p. 109°-111° C. (from ethyl acetate). Found: C, 63.80; H, 6.40; N, 13.87. C16H19N3O3 requires: C, 63.77; H, 6.36; N, 13.94%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04636500 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-1704bf9fff134f6286bc8616b5738600 |
| Source note | uspto-grants-1987_01 |