HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfate Ion → H 142-08
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfate Ion | HCID 1117 | — |
| Reactant | N-(2-Aminoethyl)-4-morpholinecarboxamide | HCID 11041198 | — |
| Reactant | 4-(2-(2-Methylpropoxy)ethoxy)phenoxy-1,2-epoxypropane | HCID 86741208 | — |
| Product | H 142-08 | HCID 132688 | — |
Reaction Steps
N-(2-((2-hydroxy-3-(4-(2-(2-methylpropoxy)ethoxy)phenoxy)propyl)amino)ethyl)-4-morpholinecarboxamide was prepared in accordance with example 4 using 10.1 g of the neutral sulphate of N-2-aminoethyl-4-morpholinecarboxamide and 9.3 g of 3-(4-(2-(2-methylpropoxy)ethoxy)phenoxy-1,2-epoxypropane as starting materials. Yield 3.9 g. Melting point 95°-96° C. (base). The structure was determined using NMR-analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04636501 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-175129d99d69472388166a067bfe375b |
| Source note | uspto-grants-1987_01 |