HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxirane, [[4-[2-(2-methylpropoxy)ethoxy]phenoxy]methyl]- → HCID 70438774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxirane, [[4-[2-(2-methylpropoxy)ethoxy]phenoxy]methyl]- | HCID 10635469 | — |
| Reactant | Urea, N-(2-aminoethyl)-N'-methyl- | HCID 11857456 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 70438774 | HCID 70438774 | — |
Reaction Steps
10.6 g of 3-(4-(2-(2-methylpropoxy)ethoxy)phenoxy)-1,2-epoxypropane and 14 g of N-2-aminoethyl-N'-methyl-urea was refluxed 40 h in isopropanol. The product crystallized when the heating was stopped. Recrystallized from isopropanol. Yield 8 g. M.p. 121° C. (base). The structure was determined using NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04636501 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-096c1730d29542e1964ef072ab8f057d |
| Source note | uspto-grants-1987_01 |