HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2(1H)-pyrimidinone → HCID 12795555, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2(1H)-pyrimidinone | HCID 108578 | — |
| Reactant | 2-Bromo-1-(2,4-dimethylphenyl)ethanone | HCID 2063450 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 12795555 | HCID 12795555 | — |
Reaction Steps
A mixture of 5-chloropyrimidin-2-one (425 mg) and 2-bromo-2',4'-dimethylacetophenone (682 mg) in triethylamine (1 ml) and ethanol (20 ml) was stirred at ambient temperature for 2 hours. The reaction mixture was diluted with water and the solid filtered off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04636509 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-5540877b26224e8b828787a6ee261479 |
| Source note | uspto-grants-1987_01 |