HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178522556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Trifluoroacetate | HCID 84468 | — |
| Reactant | HCID 178454163 | HCID 178454163 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178522556 | HCID 178522556 | 150.1% |
Reaction Steps
Using the procedure of Example 14, 7.8 g of the product of Example 11, 80 ml of methylene chloride, and 40 ml of trifluoroacetic acid were reacted to obtain 8.0 g of 4-hydroxy-2-[(2S) 2-pyrrolidinyl]-N-(2-thiazolyl)-8-trifluoromethyl-3-quinoline carboxamide in the form of its trifluoroacetate melting at 210° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04636512 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-00eae502ec2d469f8e93150052ad87b1 |
| Source note | uspto-grants-1987_01 |