HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propyl mercaptan → HCID 13784989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propyl mercaptan | HCID 7848 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1,2-Dibromo-1,1,2,2-tetrafluoroethane | HCID 31301 | — |
| Reactant | 4-Amino-2,6-dichlorophenol | HCID 80037 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13784989 | HCID 13784989 | — |
Reaction Steps
In a manner similar to Step A of Example 1, the reaction of 12.5 g 0.07 mole) 4-amino-2,6-dichlorophenol, 7.3 g (0.053 mole) potassium carbonate, 1.0 g (0.013 mole) propanethiol, 36.5 g (0.14 mole) 1,2-dibromotetrafluoroethane and 125 ml of N,N-dimethylformamide produced 3.7 g of 4-(2-bromo-1,1,2,2-tetrafluoroethoxy)-3,5-dichloroaniline as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04636523 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-21f3c1a04133482889c3b90baf73b12e |
| Source note | uspto-grants-1987_01 |