HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 12822509, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Benzyl chloroformate | HCID 10387 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 12822473 | HCID 12822473 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 12822509 | HCID 12822509 | — |
Reaction Steps
Benzyl chloroformate (1.1 ml) was added to a stirred, ice-cooled solution of N-[[3-[2-(methylamino)ethyl]-1H-indol-5-yl]methyl]methanesulphonamide (1.3 g) and diisopropylethylamine (1.5 ml) in dry THF (40 ml). After 1/2 h, water (3 ml) was added and the stirring was continued for 1 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04636521 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-a52043632f24451fb5ad00d6d75ce6cf |
| Source note | uspto-grants-1987_01 |