HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(4-nitrobenzyl)methanesulfonamide → HCID 12822521, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(4-nitrobenzyl)methanesulfonamide | HCID 12822520 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium monoxide | HCID 5083724 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 12822521 | HCID 12822521 | — |
Reaction Steps
A solution of N-[(4-nitrophenyl)methyl]methanesulphonamide (2.5 g) in a mixture of ethanol (90 ml) and ethyl acetate (90 ml) was hydrogenated at room temperature and pressure over palladium oxide on charcoal (10%; 50% paste with water, 1 g) until uptake of hydrogen ceased (15 min., 820 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04636521 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-42ecaf5cc314497ba61cf02453a6baf6 |
| Source note | uspto-grants-1987_01 |