HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13107038, compound → 2,6-Di-tert-butyl-4-(5-ethyl-1H-imidazol-4-yl)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13107038 | HCID 13107038 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2,6-Di-tert-butyl-4-(5-ethyl-1H-imidazol-4-yl)phenol | HCID 13754318 | 49.8% |
Reaction Steps
By following the same procedure as in Example 17 using 2 g of 4-(3,5-di-tert-butyl-4-hydroxyphenyl)-5-ethyl-2-thioxo-4-imidazoline, 50 ml of absolute ethanol, and 1 g of a Raney nickel catalyst and recrystallizing the reaction product from toluene, 0.9 g of 4-(3,5-di-tert-butyl-4-hydroxyphenyl)-5-ethylimidazole was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04636516 |
| Source dataset | uspto-grants-1987_01 |
| ORD ID | ord-8cca0cf512e84647815724ea5ec268b1 |
| Source note | uspto-grants-1987_01 |